Raman spectroscopy of carbon nano-particles synthesized by laser ablation of graphite in water

Authors

  • J.F. Cardenas
  • T. Cadenbach
  • Z.-B. Zhang
  • C. Costa-Vera
  • A. Debut
  • A.V. Vaca
  • S.-L. Zhang
  • J.L. Paz

Keywords:

Raman spectroscopy, carbon nanoparticle, laser ablation, high resolution electron microscopy, atomic force microscopy

Abstract

Carbon nanoparticles (CNPs) have been synthesized by laser ablation of polycrystalline graphite in water using a pulsed Nd:YAG laser (1064 nm) with a width of 8 ns. Structural and mesoscopic characterization of the CNPs in the supernatant by Raman spectroscopy provide evidence for the presence of mainly two ranges of particle sizes: 1-5 nm and 10-50 nm corresponding to amorphous carbon and graphite NPs, respectively. These results are corroborated by complementary characterization using atomic force microscopy (AFM) and transmission electron microscopy (TEM). In addition, large (10-100 $ \mu $m) graphite particles removed from the surface are essentially unmodified (in structure and topology) by the laser as confirmed by Raman analysis.

Downloads

Download data is not yet available.

Downloads

Published

2017-01-01

How to Cite

[1]
J. Cardenas, “Raman spectroscopy of carbon nano-particles synthesized by laser ablation of graphite in water”, Rev. Mex. Fís., vol. 63, no. 1 Jan-Feb, pp. 71–0, Jan. 2017.