Experimental and optimization investigations of multi cycle interrupted borocarburizing process
DOI:
https://doi.org/10.31349/RevMexFis.72.041007Keywords:
boriding, microhardness, microstructure, borocarburizing, strengthAbstract
Multi cycle interrupted borocarburizing, a modified pack boriding technique, enhances AISI 1015 steel by improving strength while maintaining surface microhardness. Using response surface methodology, the effects of temperature, time, and cycles on microhardness and tensile strength were optimized. A regression model based on central composite design showed strong experimental agreement. The Multi cycle interrupted borocarburized layers exhibited distinct iron boride and carburized zones, with microhardness values of 1410HV0.05 in the iron boride zone, 650HV0.05 in the carburized zone, and 210HV0.05 in the base metal. Unlike continuous boriding, multi cycle borocarburized layers showed no needle-like structure and had a gradual hardness gradient. The X ray diffraction analysis revealed Fe3C, Fe2B, and FeB phases. The multi cycle interrupted borocarburized process achieved a 1.23 times improvement in tensile strength (488 MPa vs. 395.8 MPa). This study demonstrates multi cycle borocarburized process superiority in balancing ultimate tensile strength and microhardness compared to continuous pack boriding.
Downloads
References
S. A. Kusmanov, I. V. Tambovskiy, V. S.Sevostyanova,S. V. Savushkina, and P. N. Belkin, Surf. Coat. Technol. 291 (2016) 334. https://doi.org/10.1016/j.surfcoat.2016.02.062 DOI: https://doi.org/10.1016/j.surfcoat.2016.02.062
R. Nora, T. M. Zine, K. Abdelkader, Y. Kadi, O.Ali, and X. Jiang, Matéria (Rio J.) 24 (2019) e12327. https://doi.org/10.1590/S1517-707620190001.0609 DOI: https://doi.org/10.1590/s1517-707620190001.0609
A. K. Rai, N. Vijayashanthi, H. Tripathy,R. N. Hajra, S. Raju, S. Murugesan, and S. Saroja, J. Nucl. Mater. 495 (2017) 58. https://doi.org/10.1016/j.jnucmat.2017.08.011 DOI: https://doi.org/10.1016/j.jnucmat.2017.08.011
M. Prince, G. S. Raj, D. Y. Kumar, and P. Gopalakrishnan, High Temp. Mater. Process. 26 (2022) 1. https://doi.org/10.1615/HighTempMatProc.2022041805 DOI: https://doi.org/10.1615/HighTempMatProc.2022041805
P. Jurˇci andM.Hudáková,Mater.Perform.Charact.9 (2020)339.https://doi.org/10.1520/MPC20190086 DOI: https://doi.org/10.1520/MPC20190086
E. Hernandez-Sánchez, Y. M. Domínguez Galicia, C. Orozco-Álvarez, R. Carrera-Espinoza, H. Herrera-Hernández, and J. C. Velázquez, Adv. Mater. Sci. Eng. 2014 (2014) 249174. https://doi.org/10.1155/2014/249174 DOI: https://doi.org/10.1155/2014/249174
R. A. García-León, J. Martínez-Trinidad, R. Zepeda-Bautista, I. Campos-Silva, A. Guevara Morales, J. Martínez-Londoño, and J. Barbosa Saldaña, Tribol. Int. 157 (2021) 106885. https://doi.org/10.1016/j.triboint.2021.106885 DOI: https://doi.org/10.1016/j.triboint.2021.106885
K. Rayane, O. Allaoui, and A. Allaoui, Acta Phys. Pol. A 132 (2017) 521. https://doi.org/10.12693/APhysPolA.132.521 DOI: https://doi.org/10.12693/APhysPolA.132.521
M. Prince and A. J. Thanu, High Temp. Mater. Process. 23 (2019) 1. https://doi.org/10.1615/HighTempMatProc.2019030266 DOI: https://doi.org/10.1615/HighTempMatProc.2019030266
K. M. Winter, J. Kalucki, and D. Koshel,in Thermochemical Surface Engineering of Steels, Woodhead Publishing (2015) p. 141. https://doi.org/10.1533/9780857096524.1.141 DOI: https://doi.org/10.1533/9780857096524.1.141
D.A.Santana,G.Y.Koga,W.Wolf,I.A.Bataev,A.A. Ruktuev,C.Bolfarini,C.S.Kiminami,W.J.Botta,and A.M.JorgeJr., Surf.Coat.Technol. 386(2020)125466. https://doi.org/10.1016/j.surfcoat.2020.125466 DOI: https://doi.org/10.1016/j.surfcoat.2020.125466
I. Campos-Silva, M. Flores-Jiménez, D. Bravo Bárcenas, H. Balmori-Ramírez, J. Andraca Adame, J. Martínez-Trinidad, and J. A. Meda Campaña, Surf. Coat. Technol. 309 (2017) 155. https://doi.org/10.1016/j.surfcoat.2016.11.054 DOI: https://doi.org/10.1016/j.surfcoat.2016.11.054
M. Prince, S. L.Arjun, G. S. Raj, andP.Gopalakrishnan, Mater. Today Proc. 5 (2018) 25276. https://doi.org/10.1016/j.matpr.2018.10.330 DOI: https://doi.org/10.1016/j.matpr.2018.10.330
M. Kulka, N.Makuch, P. Dziarski, D.Mikołajczak, and D. Przestacki, Opt. Lasers Eng. 67 (2015) 163. https://doi.org/10.1016/j.optlaseng.2014.11.015 DOI: https://doi.org/10.1016/j.optlaseng.2014.11.015
P. Gopalakrishnan, S. S. Ramakrishnan, P. Shankar, and M. Palaniappa, Metall. Mater. Trans. A33 (2002) 1475. https://doi.org/10.1007/s11661-002-0070-0 DOI: https://doi.org/10.1007/s11661-002-0070-0
A. Calik, N. Ucar, A. Kocaslan, and S. Karakas, Surf. Rev. Lett. 25 (2018) 1950022. https://doi.org/10.1142/S0218625X19500227 DOI: https://doi.org/10.1142/S0218625X19500227
I.G.Sizov,U.L.Mishigdorzhiyn, andI.P.Polyansky, in Encyclopedia of Iron, Steel and Their Alloys(2016) p.346. https://doi.org/10.1081/E-EISA-120049887 DOI: https://doi.org/10.1081/E-EISA-120049887
A. Günen, E. Kanca, M. Demir, Y. Er, G. Sa˘glam, and M. S. Gök, Tribol. Trans. 60 (2017) 267. https://doi.org/10.1080/10402004.2016.1159359 DOI: https://doi.org/10.1080/10402004.2016.1159359
L.G.Vanegas,M.C.Espinosa,N.L.Perrusquia,M. A. Ruiz, V. H. Domínguez, L. H. Ramírez, and L.Melo-Máximo, Microsc.Microanal. 27 (2021) 3406. https://doi.org/10.1017/S1431927621011703 DOI: https://doi.org/10.1017/S1431927621011703
M. Mathew and P. K. Rajendrakumar, Mater. Manuf. Process. 29 (2014) 1073. https://doi.org/10.1080/10426914.2014.901538 DOI: https://doi.org/10.1080/10426914.2014.901538
M. Kheyrodin, A. Habibolahzadeh, and S. Y. B.Mousavi, Prot. Met. Phys. Chem. Surf. 53 (2017) 105. https://doi.org/10.1134/S2070205117010117 DOI: https://doi.org/10.1134/S2070205117010117
A. Erdogan, J. Tribol. 141 (2019) 121702. https://doi.org/10.1115/1.4044859 DOI: https://doi.org/10.1115/1.4044859
A. P. Krelling, C. E. Da Costa, J. C. G. Milan,and E. A. S. Almeida, Tribol. Int. 111 (2017) 234. https://doi.org/10.1016/j.triboint.2017.03.017 DOI: https://doi.org/10.1016/j.triboint.2017.03.017
A. I. Khuri, BiometricsBiostat. Int. J. 5 (2017) 87. https://doi.org/10.15406/bbij.2017.05.00133 DOI: https://doi.org/10.15406/bbij.2017.05.00133
D.C.Montgomery ,Design and Analysis of Experiments, John Wiley & Sons (2017).
T. Turkoglu and I. Ay, Int. J. Optim. Control Theor. Appl. 9 (2019) 39. https://doi.org/10.11121/ijocta.01.2019.00660 DOI: https://doi.org/10.11121/ijocta.01.2019.00660
P. D. Babu, G. Buvanashekaran, and K. R. Balasubramanian, Tribol. Trans. 58 (2015) 602. https://doi.org/10.1080/10402004.2014.998356 DOI: https://doi.org/10.1080/10402004.2014.998356
S.C.Atul,Int.J.ChemtechRes.9(2016)82.
J. L. Arguelles-Ojeda, A. Márquez-Herrera, A. L. Saldaña-Robles, A. Saldana-Robles, M. A. Corona Rivera, and J.Moreno-Palmerin, Rev.Mex. Fís. 63 (2017)76. https://doi.org/10.31349/RevMexFis.63.1.76 DOI: https://doi.org/10.31349/RevMexFis.63.1.76
S. Sashank, P. D. Babu, and P. Marimuthu, Surf. Coat. Technol. 363 (2019) 255. https://doi.org/10.1016/j.surfcoat.2019.02.036 DOI: https://doi.org/10.1016/j.surfcoat.2019.02.036
M.A.Alam, H.Y.Hamdan,M.Azeem, P.B.Hussain, M. S. bin Salit, R. Khan, S. Arif, and A.H. Ansari, J.Mater. Res. Technol. 9 (2020) 14036. https://doi.org/10.1016/j.jmrt.2020.09.087 DOI: https://doi.org/10.1016/j.jmrt.2020.09.087
A.K.Litoria,C.A.Figueroa,L.T.Bim,C. I.Pruncu, A.A.Joshi,andS.S.Hosmani,Philos.Mag.100(2020) 353. https://doi.org/10.1080/14786435.2019.1680890 DOI: https://doi.org/10.1080/14786435.2019.1680890
Z.N.AbdellahandM.Keddam,Mater. Technol. 48 (2014)237.
A. Milinovi´c, V. Maruši´c, P. Konjati´c, and N. Beri´c, Materials 15 (2022) 1858. https://doi.org/10.3390/ma15051858 DOI: https://doi.org/10.3390/ma15051858
J. Lentz, A. Rottger, F. Großwendt, and W. Theisen, ¨ Mater. Des. 156 (2018) 113 DOI: https://doi.org/10.1016/j.matdes.2018.06.040
Downloads
Published
Issue
Section
License
Copyright (c) 2026 G. Surya Raj, M. Prince

This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.
Authors retain copyright and grant the Revista Mexicana de Física right of first publication with the work simultaneously licensed under a CC BY-NC-ND 4.0 that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.